Kornblum, Nathan published the artcileThe reaction of silver nitrite with α-halo esters, Recommanded Product: Ethyl 2-Iodopropionate, the publication is Journal of the American Chemical Society (1955), 6654-5, database is CAplus.
MeCHICO2Et (I), b7 49°, nD20 1.4963, (68.7 g.) added dropwise with stirring to 92.4 g. AgONO suspended in 500 cc. dry Et2O during 1.5 h., the mixture stirred 48 h. at room temperature, and filtered, the filter residue washed with dry Et2O, the combined filtrate and washings evaporated, and the residual pale blue oil distilled yielded 35.3 g. MeCH(NO2)CO2Et, b9 75-6°, nD20 1.4210; it was readily recovered in 90% yield from a solution in saturated aqueous NaHCO3 by acidification with aqueous AcOH containing urea. ICH2CO2Et, b3 60° nD20 1.5045, yielded similarly during 48 h. 77% O2NCH2CO2Et, b3 71-2°, nD20 1.4245. EtCHICO2Et, b1 46°, nD20 1.4923, gave in the same manner during 54 h. 75% EtCH(NO2)CO2Et, b8 82-3%, nD20 1.4233. BuCHICO2Et, b4 84°, nD20 1.4873, gave during 144 h. 84% BuCH(NO2)CO2Et, b3 80-1°, nD20 1.4302. Me2CHI (5.95 g.) and 200 cc. Et2O stirred with cooling in ice, after 1 h. 1-cc. samples in duplicate withdrawn to give the initial concentration of iodide, the solution treated with 53.9 g. AgONO as rapidly as possible, and the reaction followed by converting the unreacted Me2CHI in 1-cc. aliquots with Raney Ni to ionic iodide and titrating as such with AgNO3; the reaction was 50% completed in 8 min. The similar reaction of I with AgONO was 50% over in 4860 min. BrCH2CO2Et (50.1 g.) treated 6.5 days with 48.5 g. AgONO at 25-8° gave 40.1 g. unreacted I.
Journal of the American Chemical Society published new progress about 31253-08-4. 31253-08-4 belongs to iodides-buliding-blocks, auxiliary class Iodide,Ester, name is Ethyl 2-Iodopropionate, and the molecular formula is C5H9IO2, Recommanded Product: Ethyl 2-Iodopropionate.
Referemce:
https://en.wikipedia.org/wiki/Iodide,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com