Electric Literature of 19099-54-8, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 19099-54-8, name is 1-Iodo-2-isopropylbenzene, This compound has unique chemical properties. The synthetic route is as follows.
0.3 mmol of sodium carbonate, 0.1 mmol of 1,2-bis(3-methoxyphenyl)acetylene, 0.005 mmol of palladium acetate, and double (2-0.005 mmol of diphenylphosphoryl phenyl)ether, 0.15 mmol of pinacol borate, 0.15 mmol of 2-isopropyliodobenzene and N,N-1 mL of methylformamide was added to a 15 mL reaction tube, nitrogen was repeatedly filled 10 times, placed in an oil bath at 120 C, and reacted for 24 hours;Cool to room temperature, dilute with ethyl acetate, wash three times with water, dry with organicNa2SO4 is dried, filtered, concentrated, thin layerChromatography purification gave 20.8 mg of the desired product in a yield of 43%. The nuclear magnetic and high resolution mass spectra of this compound are characterized as follows:
The chemical industry reduces the impact on the environment during synthesis 1-Iodo-2-isopropylbenzene. I believe this compound will play a more active role in future production and life.
Reference:
Patent; Huaqiao University; Cheng Guolin; Lv Weiwei; (10 pag.)CN109879899; (2019); A;,
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