19094-56-5, Name is 2-Chloro-5-iodobenzoic acid, molecular formula is C7H4ClIO2, belongs to iodides-buliding-blocks compound, is a common compound. In a patnet, author is Vlasova, N. N., once mentioned the new application about 19094-56-5, Name: 2-Chloro-5-iodobenzoic acid.
Acyl iodides in organic synthesis. reaction of acetyl iodide with Dialkyl sulfides and disulfides
Reactions of acetyl iodide with dialkyl and dialkenyl sulfides RSR (R = Et, Bu, CH2=CH, CH2=CHCH2) and with disulfides RSSR (R = Pr, C6H13, PhCH2) were studied. Dialkyl sulfides reacted with MeCOI to give the corresponding alkyl ethanethioates and alkyl iodides as a result of cleavage of the S-C bond. The reactions of acetyl iodide with divinyl and diallyl sulfides involved addition across the double bond and subsequent polymerization of 1-alkenylsulfanyl-2(3)-iodoalkyl methyl ketones. Dialkyl disulfides RSSR (R = Pr, C6H13) and dibenzyl disulfide reacted with acetyl iodide via cleavage of the S-S bond to produce the corresponding ethanethioates and organylsulfenyl iodides. The latter underwent disproportionation to form the initial disulfide and molecular iodine. DOI: 10.1134/S1070428013010090
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