Recommanded Product: 75732-01-3. The fused heterocycle is formed by combining a benzene ring with a single heterocycle, or two or more single heterocycles. Compound: Mesitylcopper(I), is researched, Molecular C9H11Cu, CAS is 75732-01-3, about Structural diversity of calcium organocuprates(I): Synthesis of mesityl cuprates via addition and transmetalation reactions of mesityl copper(I). Author is Krieck, Sven; Goerls, Helmar; Westerhausen, Matthias.
The addition of [(L)4Ca(I)Mes] (Lewis base L = thf, Et2O) to mesityl copper(I) and the transmetalation reaction of mesityl copper(I) with activated calcium are suitable pathways for the synthesis of dimesityl cuprates(I) of calcium. However, the structures of the calcium cuprates(I) depend on the preparative procedure. The transmetalation reaction leads to the formation of [Mes-Cu-Mes]- anions whereas the addition yields dinuclear [(Mes-Cu)2(μ-Mes)]- anions. The solvent-separated counterions are [Ca(thf)6]2+ and [(thf)5CaI]+, resp. In contrast to these findings, the addition of [(L)4Ca(I)Mes] to mesityl copper(I) in an Et2O/toluene mixture led to formation of tetrameric solvent-free iodocalcium dimesityl cuprate(I) [ICa(μ-η1,η6-Mes2Cu)]4, representing a rare example of a heavy Normant-type organocuprate.
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Reference:
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com