Reference of 32024-15-0, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 32024-15-0 name is 3-Iodo-4,5-dimethoxybenzaldehyde, This compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
2-Acetylnaphthalene (511 mg, 3.0 mmol) was dissolved in MeOH (10 mL) and 3-iodo-4,5-dimethoxybenzaldehyde (876 mg, 3.0 mmol) was added. 5% NaOH (3.0 mL) was added and the reaction mixture was stirred at room temperature for 16 h. The formed precipitate was collected, washed with MeOH and dried in vacuum. Yield: 1.127 g (2.54 mmol, 85%);
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 3-Iodo-4,5-dimethoxybenzaldehyde, and friends who are interested can also refer to it.
Reference:
Article; Schmitt, Florian; Draut, Heidrun; Biersack, Bernhard; Schobert, Rainer; Bioorganic and Medicinal Chemistry Letters; vol. 26; 21; (2016); p. 5168 – 5171;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com